Metal-free remote site-selective radical C(sp 3 )–H acyloxylation of amides

作者：Yan‐Shuo Zhu, Wenya Zhang, Hongyan Wang, Dan Li, Xinxin Xie, Hongwei Hu, Penghua Shu · 发表于：New Journal of Chemistry · 年份：2025 · DOI：10.1039/d5nj00098j · 被引用次数：4 · 研究领域：Catalytic C–H Functionalization Methods、Advanced Synthetic Organic Chemistry、Radical Photochemical Reactions

Here, we report a method for the direct acyloxylation of C(sp 3 )–H bonds employing photo-induced and the 1,5-HAT process. This approach features broad substrate scope, excellent functional group compatibility, and complete regioselectivity.