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[Influence of different amount of silane coupling agent on the flexural strength of PMMA/nanometer ZrO2 composites].

作者:Yi-ming Bian, Xiuyin Zhang, Bangshang Zhu, Weiqiang Yu, Dan-ping Ruan, Min Min · 发表于:PubMed · 年份:2007 · 被引用次数:6 · 研究领域:Dental materials and restorations、Dental Implant Techniques and Outcomes、Endodontics and Root Canal Treatments

PURPOSE: To study the influence of different amount of silane coupling agent Z-6030 on the flexural strength of PMMA/nanometer ZrO(2) composites. METHODS: Nanometer ZrO(2) particles were modified by silane coupling agent Z-6030 with different percentages.In situ polymerization method was used to combine PMMA/ nanometer ZrO(2) composites of denture base plate. With reference to the standard of ISO1567:1999, standard samples of the experimental group were made. PMMA II type powder and PMMA II type liquor were used,which was not added nanometer ZrO(2) and silane coupling agent to make the standard samples of common denture base plate. PMMA II type powder and PMMA II type liquor were used,which was added nanometer ZrO(2) unmodified by silane coupling agent to make the standard samples of the control group. The data of flexural strength of the base plate materials were tested with three-point bending test. One-way ANOVA was adopted to analyze the data using SAS 6.12 software package. RESULTS: When the percentage of silane coupling agent Z-6030 was 3.5%,the flexural strength of PMMA/nanometer ZrO(2) composite resin material of denture base plate was strongest, which was significantly higher than that of the common denture base plate group,the control group,2.0% group,4.0% group,4.5% group and 5.0% group(P<0.05). 0.5% group,1.0% group,1.5% group,2.5% group,3.0% group and 3.5% group had no significant difference with each other(P>0.05). 0.5% group,1.0% group,1.5% group,2.0% group,2.5...