The deformation-DIA: A new apparatus for high temperature triaxial deformation to pressures up to 15 GPa

作者：Yanbin Wang, W. B. Durham, Ivan C. Getting, Donald J. Weidner · 发表于：Review of Scientific Instruments · 年份：2003 · DOI：10.1063/1.1570948 · 被引用次数：289 · 研究领域：High-pressure geophysics and materials、Boron and Carbon Nanomaterials Research、Diamond and Carbon-based Materials Research

A new deformation apparatus has been developed, based on the widely used cubic-anvil apparatus known as the DIA. Two differential rams, introduced in the upper and lower guide blocks, allow independent control of the differential strain and stress field under high confining pressure. Testing experiments with synchrotron x rays have demonstrated that this deformation DIA (D-DIA) is capable of generating up to 30% axial strain on a 1–2 mm long sample under confining pressures up to 15 GPa at simultaneous high temperatures. Various compressional strain rates from 10−3 to about 5×10−6 s−1 have been achieved. Extensional experiments have also been carried out successfully. Strains are measured by x-ray imaging of the sample which has a length measurement precision of ∼0.1 μm; pressures are monitored using standard materials with well established equations of state. X-ray transparent anvils made of sintered polycrystalline cubic boron nitride have been successfully tested, with a two-dimensional x-ray charge coupled device detector. Distortions in the diffraction lines due to differential stress can be measured with a precision of about 20 MPa.